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Title of Journal: J Supercond Nov Magn

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Abbravation: Journal of Superconductivity and Novel Magnetism

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Springer US

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DOI

10.1007/bf00642108

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ISSN

1557-1947

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Synthesis of Superparamagnetic NiSubscript040/

Authors: Manoj M Kothawale R B Tangsali G K Naik J S Budkuley
Publish Date: 2015/04/14
Volume: 28, Issue: 8, Pages: 2461-2463
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Abstract

The powder of Ni 040Zn 060Fe 2 O 4 nanoparticles is synthesized using a microwaveassisted combustion method Xray diffraction and IR spectrum analysis show that the sample has a singlephase spinel structure Debye–Scherrer formula reveals a crystallize size of 49 nm ±5 whereas transmission electron microscopy TEM results show particle sizes in the range of 10 to 60 nm Superparamagnetic nature of the sample was confirmed from a close hysteresis loop The Curie temperature T C was found to be 422 ∘C and 30 K as a blocking temperature

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