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Title of Journal: Catal Lett

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Abbravation: Catalysis Letters

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Springer US

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DOI

10.1007/bf02677909

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1572-879X

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Mechanochemical Synthesis and Electrochemical Char

Authors: L John Berchmans R Karthikeyan M Helan Sheela Berchmans V Ŝepelak K D Becker
Publish Date: 2011/06/08
Volume: 141, Issue: 10, Pages: 1451-1457
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Abstract

The studies on the mechanochemical synthesis and electrochemical characterization of orthorhombic calcium ferrite CaFe2O4 are reported in this paper Stoichiometric mixtures of αFe2O3 and granulated Ca metal were used as the starting materials for the synthesis process The synthesized calcium ferrite was characterized by roomtemperature Mössbauer spectra XRD and TEM The electrochemical characterisation was carried out using cyclic voltammetry studies Mössbauer spectra provide the yield of the reaction information on the charge status the local symmetry and the magnetic state of the iron ions in the mechanosynthesized ferrite material XRD analysis of the CaFe2O4 compound reveals the orthorhombic crystal structure with an average crystalline size of about 28 nm TEM micrographs reveal the nanoparticles with irregular crystal morphology ranging from 8 to 30 nm The electrochemical studies clearly show that the calcium ferrite compound can act as an electrocatalyst for Oxygen Evolution Reaction OERThe authors sincerely thank for the financial support given by German Academic Exchange ServiceDAAD—Germany Department of Science and Technology DST New Delhi India and Council of Scientific and Industrial Research CSIR New Delhi India to carry out this study

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  1. Synthesis and Catalytic Performance of ZSM-5/MCM-41 Zeolites With Varying Mesopore Size by Surfactant-Directed Recrystallization
  2. Oxygen-Nonstoichiometric YBaCo 4 O 7+δ as a Catalyst in H 2 O 2 Oxidation of Cyclohexene
  3. Enhanced Low-Temperature Activity of Ag-Promoted Co-ZSM-5 for the CH 4 -SCR of NO
  4. Hydrogenation of m -Dinitrobenzene Over Pt Supported Catalysts on TiO 2 –Al 2 O 3 Binary Oxides
  5. Synthesis of Two Novel Water-Soluble Iron Phthalocyanines and Their Application in Fast Chromogenic Identification of Phenolic Pollutants
  6. Metal Support Interactions in Co 3 O 4 /Al 2 O 3 Catalysts Prepared from w/o Microemulsions
  7. Effect of CeO 2 Doping on Structure and Catalytic Performance of Co 3 O 4 Catalyst for Low-Temperature CO Oxidation
  8. Application of Inelastic Neutron Scattering to the Methanol-to-Gasoline Reaction Over a ZSM-5 Catalyst
  9. Catalytic Method for N -Methyl-4-pyridone Synthesis in the Presence of ZnAl 2 O 4
  10. Oxidation of Olefins Using Rhenium Supported by Imidazole-Functionalized Amphiphilic Copolymers
  11. Radiochromatographic studies of isobutylene oxidation over SnO 2
  12. Effect of Enhanced Support Acidity on the Sulfate Storage and the Activity of Pt/γ-Al 2 O 3 for NO Oxidation and Propylene Oxidation
  13. Synthesis, Characterization and Catalytic Properties of Chiral BINOL Functionalized Mesoporous Silicas for Enantioselective Morita-Baylis-Hillman Reaction
  14. Effect of Mg Addition on the Physical and Catalytic Properties of Cu/CeO 2 for NO + CO Reduction
  15. Deep HDS of Diesel Fuel: Inhibiting Effect of Nitrogen Compounds on the Transformation of the Refractory 4,6-Dimethyldibenzothiophene Over a NiMoP/Al 2 O 3 Catalyst
  16. Preparation, Characterization and Reactivity of Keggin Type Phosphomolybdates, H 3−2 x Ni x PMo 12 O 40 and (NH 4 ) 3−2 x Ni x PMo 12 O 40 , for Adipic Acid Synthesis
  17. Functionalized Poly(ethylene glycol)-Stabilized Palladium Nanoparticles as an Efficient Catalyst for Aerobic Oxidation of Alcohols in Supercritical Carbon Dioxide/Poly(ethylene glycol) Biphasic Solvent System
  18. Synthesis of CaIn 2 O 4 Rods and Its Photocatalytic Performance Under Visible-light Irradiation
  19. Glycerol hydrogenolysis to propylene glycol
  20. Glycothermal Synthesis and Catalytic Properties of Nanosized Zn 1− x Co x Al 2 O 4 ( x = 0, 0.5, 1.0) Spinels in Phenol Methylation
  21. Fe 3 O 4 Nanoparticles-Supported Palladium-Bipyridine Complex: Effective Catalyst for Suzuki Coupling Reaction
  22. Cluster Structure and Reactions: Gaining Insights into Catalytic Processes
  23. Hydrocracking and Hydroisomerization of n -Hexadecane, n -Octacosane and Fischer–Tropsch Wax Over a Pt/SiO 2 –Al 2 O 3 Catalyst
  24. Reduction of Ketones with Silanes Catalysed by a Cyclopentadienyl-Functionalised N -Heterocyclic Iron Complex
  25. The First Case of Competitive Heterogeneously Catalyzed Hydrogenation using Continuous-Flow Fixed-Bed Reactor System: Hydrogenation of Binary Mixtures of Activated Ketones on Pt-Alumina and on Pt-Alumina-Cinchonidine Catalysts
  26. Steam reforming of ethanol on Ni–CeO 2 –ZrO 2 catalysts: Effect of doping with copper, cobalt and calcium
  27. Different Catalytic Reactions of n -Hexane and 1-Hexene on Molybdenum Based Catalysts
  28. Palladium-Schiff Base Complex Immobilized Covalently on Magnetic Nanoparticles as an Efficient and Recyclable Catalyst for Heck and Suzuki Cross-Coupling Reactions
  29. From Gas to Liquid Phase Sulfidation: An IR Spectroscopy Study
  30. “An American Scientist: The Autobiography of Gabor A Somorjai with Mitch Jacoby”
  31. Low-Temperature CO Oxidation of Gold Catalysts Loaded on Mesoporous TiO 2 Whisker Derived from Potassium Dititanate
  32. Hydrogen Production by Steam Reforming of Liquefied Natural Gas over Mesoporous Ni-Al 2 O 3 Catalysts Prepared by a Co-Precipitation Method: Effect of Ni/Al Atomic Ratio
  33. Liquid-Phase Selective Hydrogenation of 1-Heptyne over Pd/TiO 2 Catalyst Synthesized by One-Step Flame Spray Pyrolysis
  34. Nanocatalysis I: Synthesis of Metal and Bimetallic Nanoparticles and Porous Oxides and Their Catalytic Reaction Studies
  35. Copper-Catalysed One-Pot Synthesis of 2,3,4,9-Tetrahydro-1 H -Xanthen-1-Ones from 2-Halobenzylbromides and Cyclic-1,3-Diketones in Water
  36. Selective hydrogenolysis of glycerol to propylene glycol on Cu–ZnO catalysts
  37. Reduction of N -(alkoxy(aryl)methyl)benzamide Compounds by a Hantzsch Ester 1,4-Dihydropyridine Using Pd/C as a Catalyst
  38. Role of Baria Dispersion in BaO/Al 2 O 3 Catalysts for Transesterification
  39. Peculiarities of dehydroaromatization of CH 4 –C 2 H 6 and CH 4 over Mo/ZSM-5 catalysts
  40. Properties and Catalytic Performance for Methane Combustion of LaMnO 3 Perovskite Prepared in Oil–Water Two-phase System
  41. Dealumination of Zeolite Beta Catalyst Under Controlled Conditions for Enhancing its Activity in Acylation and Esterification
  42. Preparation and catalytic activity of a new dioxomolybdenum(VI) complex for olefin epoxidation
  43. Preparation of La-Mn-O Perovskite Catalyst by Microwave Irradiation Method and its Application to Methane Combustion
  44. Low Temperature NO Storage of Zeolite Supported Pd for Low Temperature Diesel Engine Emission Control
  45. A Cu Nanoparticle Embedded in Electrospundoped Carbon Nanofibers as Efficient Catalysts for Ullmann O-Arylation of Aryl Halides with Various Phenols
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  47. Nanostructured Cu-Doped Ceria Obtained by Reverse Microemulsion Method as Catalysts for Incineration of Selected VOCs
  48. A Fine Dispersed Cobalt Catalyst with Macro-Pore for Hydroformylation of 1-Hexene
  49. Dialkylation of Naphthalene with Isopropanol Over H 3 PO 4 /MCM-41 Catalysts for the Environmentally Friendly Synthesis of 2,6-Dialkylnaphthalene
  50. Synthesis, Characterization and Catalytic Application of MCM 41 Supported Phenanthrolinium Dibromide Catalyst for Aza-Michael Addition Reaction in Aqueous Medium
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  52. Mesoporous SBA-15 with Short Mesochannels Immobilized Natural Quinine for Asymmetric Michael Addition of Chalcones
  53. First Report About the Use of Micellar Keggin Heteropolyacids as Catalysts in the Green Multicomponent Synthesis of Nifedipine Derivatives
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