Authors: Akram Panjehpour Ali Morsali
Publish Date: 2012/04/10
Volume: 22, Issue: 5, Pages: 938-945
Abstract
Crystalline and nanostructure of a new PbII coordination polymer PbNO22qucn 1 Hquc = 2quinoline carboxylic acid is synthesized via heat gradient and sonochemical methods respectively The newly synthesized structures are characterized by scanning electron microscopy SEM X ray powder diffraction XRD IR and 1HNMR spectroscopies elemental analyses and single crystal Xray diffraction is used to understand the exact structure of the crystalline 1 Thermal stability of nano and bulk samples of compound 1 are studied and compared through thermal gravimetric and differential thermal analyses PbO nanoparticles are then produced by calcination of the nanostructure of compound 1 at 600 °C The obtained PbO is characterized by XRD and SEM analyses
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