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Title of Journal: Russ Chem Bull

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Abbravation: Russian Chemical Bulletin

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Springer US

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DOI

10.1016/0003-9969(70)90110-x

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ISSN

1573-9171

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Heterocyclization of hydrazine with acetaldehyde a

Authors: V R Akhmetova G R Nadyrgulova N N Murzakova Z A Starikova M Yu Antipin R V Kunakova
Publish Date: 2010/04/17
Volume: 58, Issue: 5, Pages: 1091-1093
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Abstract

Hydrazine is regioselectively condensed with a mixture of acetaldehyde and H2S at a temperature below −10 °C to form 2468tetramethyl37dithia15diazabicyclo330octane The reaction at 0 °C with the reverse order of mixing of the starting reagents affords 246trimethyl135dithiazinan5ylamine as the major product

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