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Title of Journal: Russ Chem Bull

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Abbravation: Russian Chemical Bulletin

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Springer US

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DOI

10.1016/0020-708x(83)90177-1

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ISSN

1573-9171

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Synthesis crystal structure and interconversions

Authors: V R Akhmetova Z T Niatshina G R Khabibullina I S Bushmarinov A O Borisova Z A Starikova L F Korzhova R V Kunakova
Publish Date: 2010/11/17
Volume: 59, Issue: 5, Pages: 1002-1009
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Abstract

Chemoselectivity of multicomponent reaction of anilines with the CH2OH2S thiomethylating mixture in the synthesis of Narylsubstituted 135dithiazinanes 135thiadiazinanes and 15dithia37diazacyclooctanes has been studied depending on the type and mutual arrangement of substituents in the starting anilines ratio of reagents temperature and reaction time Conformation of the synthesized heterocycles in crystal has been found by Xray diffraction Interconversion of the heterocycles showed stability of Naryl135dithiazinanes

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