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Title of Journal: J Wuhan Univ TechnolMat Sci Edit

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Abbravation: Journal of Wuhan University of Technology-Mater. Sci. Ed.

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Wuhan University of Technology

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10.1002/chin.199414127

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1993-0437

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Hydrothermal synthesis ultralong singlecrystal Sb

Authors: Yun Liu Hongyan Miao Guoqiang Tan Gangqiang Zhu
Publish Date: 2010/06/12
Volume: 25, Issue: 3, Pages: 411-414
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Abstract

This paper describes an ethylene glycol EGassisted approach to the ultralong Sb2S3 nanowires formed by a simple hydrothermal reaction between SbCl3 and Na2S in the presence of distilled water Transmission electron microscopy and scanning electron microscopy studies indicate that these Sb2S3 nanowires possess a diameter around 200 nm and length up to 100 μm Highresolution transmission electron microscopy and selected area electron diffraction studies reveal that each Sb2S3 nanowire is a singlecrystal along the 001 direction The possible formation mechanism of the nanowires was discussed The effects of volume ratio of ethylene glycol/water on the morphology of Sb2S3 nanowires were also investigated Diffuse reflectance spectrum result shows that the final products have an apparent blue shift by quantum size effect

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