Authors: Helmut Egg
Publish Date: 1975/09/01
Volume: 106, Issue: 5, Pages: 1167-1173
Abstract
As starting materials for theoretical and pharmacological studies 715diazadispiro5153hexadecane 1 its 14imino2 and 14oxoderivative 3 were prepared Reduction of bis1cyanocyclohexylamine 4 withLAH leads to a mixture of1 and2 For the exclusive preparation of1 4 is treated with conc H2SO4 to yield the corresponding 1416dioxohexadecane which is reduced to1 withLAH The preparation of3 is effected by acid hydrolysis of acetylated2
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