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Title of Journal: Monatsh Chem

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Abbravation: Monatshefte für Chemie - Chemical Monthly

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Springer-Verlag

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DOI

10.1007/s00706-006-0560-7

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1434-4475

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The Emphasis Type="Italic"WillgerodtKindler/Em

Authors: Kioumars Aghapoor Farshid Mohsenzadeh Golriz Khanalizadeh Hossein R Darabi
Publish Date: 2007/01/02
Volume: 138, Issue: 1, Pages: 61-65
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Abstract

Water has been found for the first time as a useful solvent in the WillgerodtKindler WK reaction for the synthesis of benzothiomorpholides in high yield at 80°C for 3 h This novel approach confronts the WK protocol with a new situation in which water not only is not regarded as a serious disadvantage but also is applied in this case as a useful solvent in the reaction The basis of this finding is the presence of a methylene chain in the carbonyl substrates which leads to the high reaction selectivity of benzaldehydes over acetophenones

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  14. 4th Young Investigator Workshop
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