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Title of Journal: Bull Mater Sci

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Abbravation: Bulletin of Materials Science

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Springer-Verlag

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DOI

10.1007/s13170-014-0055-x

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0973-7669

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Gel–sol synthesis and aging effect on highly cryst

Authors: SHARIF SHAHINI MASOUD ASKARI S K SADRNEZHAAD
Publish Date: 2011/12/06
Volume: 34, Issue: 6, Pages: 1189-1195
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Abstract

Highly crystalline TiO2 anatase nanoparticles were synthesized via gel–sol method by using titanium isopropoxide and triethanolamine The products were characterized by Xray diffraction transmission electron microscopy thermogravimetric/differential thermal analysis and nitrogen gas absorption methods The particle size ranged from 7 to 24 nm having specific surface area of 64 to 220 m2/g Selective TiOH4 gel specifications and hydrothermal test conditions resulted in thermodynamicallystable phaseformation Aging at 130°C for 4 h resulted in particle size of 7 nm while at 130 and 160°C for 12 h resulted in 12 and 21 nm respectively

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