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Title of Journal: J Chem Crystallogr

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Abbravation: Journal of Chemical Crystallography

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Springer US

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DOI

10.1016/0161-5890(78)90095-0

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1572-8854

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Crystal and Molecular Structures of Di1Adamantyl

Authors: Fernando RascónCruz Sandra GonzálezGallardo Miguel A MuñozHernández Rubén A Toscano Verónica GarcíaMontalvo
Publish Date: 2009/02/26
Volume: 39, Issue: 7, Pages: 530-534
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Abstract

Synthesis and Xray structural determination of three phosphorus compounds are reported 3b is monoclinic P21/c with a = 118521 b = 128251 c = 124451 Å β = 1036931º 4a and 4b are monoclinic P21/n with a = 12142216 b = 9086012 c = 148452 Å β = 964983º for 4a and a = 12271416 b = 9281212 c = 148002 Å β = 971762º for 4b They all exhibit distorted tetrahedral geometry about the P atom Ph2PXNHC7H7 X=S 4a and X=Se 4b show typical P–S and P–Se double bond distances and P–N single bonds while P–S bond in 1Ad2PSCl 3b is comparable to P–S single bonded probably due to the largeness of 1adamantyl groups

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