Journal Title
Title of Journal: J Chem Crystallogr
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Abbravation: Journal of Chemical Crystallography
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Authors: ZhiQiang Dong FangMing Liu YongMing Zeng
Publish Date: 2011/03/30
Volume: 41, Issue: 8, Pages: 1158-1164
Abstract
A series of new heterocyclic compounds bearing 123triazole moiety were synthesized using 4acetyl2phenyl123triazole 1 as the starting material The target compounds were prepared and the structures were characterized by IR 1H NMR MS and elemental analysis Meanwhile the crystal structures of the synthesized compounds were also furthered confirmed by Xray diffraction analysis Compound 3b crystallized in the monoclinic P21/c space group with unit cell parameters a = 10697417 Å b = 203563 Å c = 7804912 Å α = 90° β = 1028403° γ = 90º V = 165715 Å3 Z = 4 T = 2932 K Compound 7c crystallized in the Triclinic P1 space group with unit cell parameters a = 73642 Å b = 73662 Å c = 260898Å α = 871147° β = 870407 3° γ = 823377° V = 139927 Å3 Z = 2 T = 2932 K Compound 10c crystallized in the Triclinic P1 space group with unit cell parameters a = 9815210 Å b = 10080613 Å c = 11126714 Å α = 1003443° β = 1119753° γ = 1078523° V = 9161819 Å3 Z = 2 T = 2932 K
Keywords:
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- Hydrogen Bonded 3D Supramolecular Architectures of Three Saccharinate Salts
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