Journal Title
Title of Journal: J Chem Crystallogr
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Abbravation: Journal of Chemical Crystallography
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Authors: Qingfu Zhang Jiandong Pang Suyuan Zeng Caihua Liu Dezhi Sun
Publish Date: 2011/12/14
Volume: 42, Issue: 3, Pages: 271-275
Abstract
A new bishydrazone compound NN′diE12hydoxyphenylmethylidene26naphthalenedicarbohydrazide 1 has been prepared by condensation reaction of 26naphthalenedicarbohydrazide with salicylaldehyde in ethanol and characterized by elemental analysis FTIR 1H and 13CNMR ESI–MS and singlecrystal Xray diffraction analysis The crystal of 1·2DMF belongs to monoclinic space group P21/n with a = 104541 b = 77111 c = 188012 Å β = 933641° V = 151293 Å3 Z = 2 D c = 1314 g cm−3 μ = 0093 mm−1 F000 = 632 Mr = 59865 the final R 1 = 00861 and wR 2 = 02279 for 7243 observed reflections with I 2σI The structural analysis reveals that compound 1·2DMF contains one NN′diE12hydoxyphenylmethylidene26naphthalenedicarbohydrazide molecule and two NNdimethylformamide solvent molecules A 2D supramolecular structure of 1·2DMF was constructed by multiple intermolecular N–H···O and C–H···O hydrogen bondsThis study was supported by the National Nature Science Foundation of China Grant No 21001061 the Nature Science Foundation of Shandong Province Grant No ZR2010BL020 and the Liaocheng University Funds for Young Scientist 31805 and also partially supported by Postgraduate Students’ Inovation Project of Shandong Province LCUYZ10008
Keywords:
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