Journal Title
Title of Journal: J Chem Crystallogr
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Abbravation: Journal of Chemical Crystallography
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Authors: Miguel Guerrero Josefina Pons Mercè FontBardia Teresa Calvet Josep Ros
Publish Date: 2011/01/13
Volume: 41, Issue: 5, Pages: 721-726
Abstract
The crystal structure of the title compound C22H30N4O2·H2O L has been determined using Xray diffraction at 293 K The crystal of 12bis435dimethyl1Hpyrazol1yl2oxobutylbenzene is in triclinic crystal system with space group P−1 Z = 2 lattice parameters a = 82256 Å b = 109676 Å c = 129036 Å V = 1119111 Å3 Analyses of single crystals of L crystallized from dichloromethane/diethyl ether 11 revealed that the molecules are arranged in couples which adopt a pseudo chair conformation by means of intermolecular O–H···N hydrogen bonding interactions Moreover the extended structure revealed a 1D chain caused by several C–H···N intermolecular interactions
Keywords:
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- Structures of Protonated Bis(pyridine-2-yl) Ketone Arylhydrazone Derivatives: [(C 5 H 4 N)(C 5 H 4 NH)C=NNHC 6 H 4 Y] + [X] − (Y,X = 3-O 2 N,Cl: 4-Me,Cl:)
- Hydrogen Bonded 3D Supramolecular Architectures of Three Saccharinate Salts
- Crystal structure of potassium tris[3-(2-pyridyl)pyrazolyl]hydroborate
- X-ray Structure Investigation of 20- O -β- d -glucopyranosyl-20( S )-protopanaxadiol
- Synthesis, X-ray Structure and Photo Chemistry of 2-(Methyl(1-Phenylvinyl)Carbamoyl)Phenyl Acetate
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