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Title of Journal: J Chem Crystallogr

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Abbravation: Journal of Chemical Crystallography

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Springer US

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DOI

10.1016/0378-1135(89)90080-1

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1572-8854

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Unusual Very Strong O–H···O Hydrogen Bonding in Zi

Authors: İbrahim Kani
Publish Date: 2012/06/21
Volume: 42, Issue: 8, Pages: 832-838
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Abstract

The centrosymmetric dimer zinc compound ZnHLbpy2H2O2L L = O2CCF26CO2 bpy = 22′bipyridine was obtained through the reaction of ZnClO42·6H2O bpy and perfluorosuberic acid ZnII centre is coordinated by four N atoms from two bpy ligands and two O atoms from a water molecule and monoanionic suberate ligand in a distorted octahedral coordination environment The unit structure contains crystallographically centrosymmetric suberate anion which acts as a bidentate bridging ligand between each cationic monomer complex unit via hydrogen bonding The very strong interaction of hydrogen bonding of hydoxycarbonyl–carboxylate system in solid state has O–H···O 24363 Å O···H = 1256 Å and H···O = 1196 Å These units are also connected to each other via π···π C–H···π C–F···π and F···F stacking interactions C–H···O O–H···O and C–H···F hydrogen bonds giving rise to a multidimensional network The complex is the first reported example of a coordination compound based on both bpy ligands together with perfluorosuberic acid Moreover compound exhibit intense solid state fluorescent emissions at room temperature


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  2. Hydrogen Bonded 3D Supramolecular Architectures of Three Saccharinate Salts
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  6. Crystal and Molecular Structures of Di-1-Adamantylthiophosphinic Chloride, P , P -Diphenyl- N -Benzyl Phosphinothioic- and Selenoic- Amides
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