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Title of Journal: J Nat Med

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Abbravation: Journal of Natural Medicines

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Springer Japan

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DOI

10.1007/978-3-642-15461-4_45

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1861-0293

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A simple and selective detection method for aristo

Authors: Takaomi Tagami Akihiro Takeda Akiko Asada Airin Aoyama Takahiro Doi Masami Kawaguchi Keiji Kajimura Yoshiyuki Sawabe Hirotaka Obana Katsuhiro Yamasaki
Publish Date: 2013/01/10
Volume: 67, Issue: 4, Pages: 838-843
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Abstract

The official Japanese method for analyzing aristolochic acid I AAI in Asiasarum root using conventional highperformance liquid chromatography HPLC is described in the Japanese Pharmacopoeia Sixteenth Edition Interfering peaks of AAI sometimes appear after HPLC analysis of crude drugs A selective analytical method is needed to determine definitively whether AAI is present in crude drugs In this study we developed a selective method that combined solidphase extraction and liquid chromatography/mass spectrometry LC/MS which may be useful for identifying AAI in crude drugs and for quality control

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