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Title of Journal: J Therm Anal Calorim

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Abbravation: Journal of Thermal Analysis and Calorimetry

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Springer Netherlands

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DOI

10.1016/0305-0491(94)90023-x

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ISSN

1572-8943

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Synthesis and thermal behaviour of silicon contain

Authors: M Padmanabha Raju S Alam
Publish Date: 2008/02/08
Volume: 91, Issue: 2, Pages: 401-404
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Abstract

A series of silicon containing polyester imides PEIs were synthesized using novel vinyl silane diester anhydride VSEA and various aromatic and aliphatic dimines by twostep process includes ringopening polyaddition reaction to form polyamic acid and thermal cyclodehydration process to obtain polyester imides VSEA was synthesized by using dichloro methylvinylsilane and trimellitic anhydride in the presence of K2CO3 by nucleophilic substitution reaction The PEIs were characterized by FTIR spectroscopy The thermal properties of PEIs were investigated by using differential scanning calorimetry DSC and thermogravimetric analysis TG methods The prepared PEIs showed glass transition temperatures in the range of 320–350°C and their 5 mass loss was recorded in the temperature range of 500–520°C in nitrogen atmosphere These had char yield in the range of 45–55 at 800°C

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  9. Investigation on the thermal decomposition some heterodinuclear Ni II -M II complexes prepared from ONNO type reduced Schiff base compounds ( M II =Zn II , Cd II )
  10. Synthesis, characterization, and thermal analysis of alginate and monoethanolamine product
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  12. Energetic study of residual forest biomass using calorimetry and thermal analysis
  13. Thermal behavior of Ca 2+ and Cu 2+ oxalates obtained by precipitation in homogeneous solution from dimethyl oxalate hydrolysis
  14. Excess enthalpies and excess volumes of binary mixtures containing a linear carboxylic acid + di- iso -propyl ether at 298.15 K and 0.1 MPa
  15. Erratum to: Thermal analysis and calorimetry in Central and Eastern Europe as a tool for solving diverse issues in different fields of science and applications
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