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Title of Journal: J Therm Anal Calorim

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Abbravation: Journal of Thermal Analysis and Calorimetry

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Springer Netherlands

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DOI

10.1016/0920-2307(92)90007-N

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ISSN

1572-8943

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A combined approach of differential scanning calor

Authors: Mohd Rushdi Abu Bakar Zoltan Kalman Nagy Christopher David Rielly
Publish Date: 2009/08/06
Volume: 99, Issue: 2, Pages: 609-619
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Abstract

A combination of differential scanning calorimetry and hotstage microscopy with image analysis has been used to investigate the polymorphism of sulfathiazole The use of light intensity profiles obtained from the HSM images as an alternative way to present results of the HSM analysis was found to be useful in describing and verifying thermal events The approach provides a unique insight into the polymorphic transformations and thermal behaviour exhibited by this compound The results of the experiments show that sulfathiazole tends to crystallise as mixtures of polymorphs even though the literature methods for producing pure polymorph were followedThe authors thank Dr David Ross of the Department of Materials Loughborough University for the use of the HSM system Financial support provided by the Engineering and Physical Sciences Research Council EPSRC UK grant EP/E022294/1 is gratefully acknowledged One of the authors MRAB is grateful to the Malaysian Ministry of Higher Education and the International Islamic University Malaysia for a scholarship

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Other Papers In This Journal:
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  2. Desorption of Water from CD/DRUG Inclusion Complexes
  3. Thermodynamics of CO probe molecule adsorption on Cu–FER-zeolite comparison of TPD, FTIR, and microcalorimetry results
  4. Oxidation studies of Indian reduced activation ferritic martensitic steel
  5. Study of the effect of tannins and animal species on the thermal stability of vegetable leather by differential scanning calorimetry
  6. Thermal conductivity of exfoliated graphite nanocomposites
  7. TG-MS analysis for studying the effects of fire retardants on the pyrolysis of pine-needles and their components
  8. Decomposition of perfluoropolyether lubricants
  9. Investigation on the thermal decomposition some heterodinuclear Ni II -M II complexes prepared from ONNO type reduced Schiff base compounds ( M II =Zn II , Cd II )
  10. Synthesis, characterization, and thermal analysis of alginate and monoethanolamine product
  11. Synthesis, characterization, and thermal analysis of alginate and monoethanolamine product
  12. Energetic study of residual forest biomass using calorimetry and thermal analysis
  13. Thermal behavior of Ca 2+ and Cu 2+ oxalates obtained by precipitation in homogeneous solution from dimethyl oxalate hydrolysis
  14. Excess enthalpies and excess volumes of binary mixtures containing a linear carboxylic acid + di- iso -propyl ether at 298.15 K and 0.1 MPa
  15. Erratum to: Thermal analysis and calorimetry in Central and Eastern Europe as a tool for solving diverse issues in different fields of science and applications
  16. Amorphous phase dynamics at the glass transition in drawn semi-crystalline polyester
  17. Calibration burning of wood crib under ISO9705 hood
  18. Influence of biomass on coal combustion based on thermogravimetry and Fourier transform infrared spectroscopy
  19. Thermal synthesis and properties of the (Bi 2 O 3 ) 1–x (Ho 2 O 3 ) x pigments
  20. Influence of the steel powder type and processing parameters on the debinding of PM compacts with gelatin binder
  21. Effect of the magnetic field on the melting transition of Ga and In by nW-stabilized DSC
  22. Isoconversional analysis of solid state transformations
  23. Investigation of copper(II) complexation by glycylglycine using isothermal titration calorimetry
  24. Flammability of diene rubbers
  25. Thermal deamination kinetics of tris(ethylenediamine)nickel(II) sulphate in the solid-state
  26. Preparation, characterization and thermal dehydration kinetics of titanate nanotubes
  27. A review on the thermal stability of calcium apatites
  28. Thermal reaction characteristics of the boron used in the fuel-rich propellant
  29. Studies of thermal decomposition kinetics and temperature dependence of thermodynamic functions of the new precursor LiNiPO 4 ·3H 2 O for the synthesis of olivine LiNiPO 4
  30. Effects of stirring rate for thermal runaway reaction in cumene hydroperoxide manufacturing process using calorimetric techniques
  31. Statistical classification of early and late wood through the growth rings using thermogravimetric analysis
  32. Conjugate heat transfer analysis of knitted fabric
  33. Erratum to: Osmo-dehydration of apple pulp studied by means of classical and Knudsen Thermogravimetric approach
  34. Influences of fly ash and fluorgypsum on the hydration heat and compressive strength of cement
  35. Thermal conductivity of lightweight aggregate based on coal fly ash
  36. Flammability studies of benzene and methanol with different vapor mixing ratios under various initial conditions
  37. Calculations of thermal functions of group-III nitrides
  38. Antioxidant activity of 6PPD derivatives in polyisoprene matrix studied by non-isothermal DSC measurements
  39. Thermal, structural analysis, Mössbauer and impedance study of copper nickel ferrite nanoparticles synthesized via Tween 80-assisted hydrothermal process
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  41. Molecular complex formation between l -phenylalanine and 18-crown-6 in H 2 O–DMSO solvents studied by titration calorimetry at T = 298.15 K
  42. Thermal treatment of pitch-polymer blends
  43. Crystallization, spectral, and thermal characterization of l -histidine methyl ester dihydrochloride (LHMED)
  44. Novel calorimetric properties of human cartilage samples in rheumatoid arthritis
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  46. Synthesis, characterization and thermal study of solid mandelate of some bivalent transition metal ions in CO 2 and N 2 atmospheres
  47. Synthesis, characterization and TG-DTA study of diethyl 5-(4-hydroxyethoxyphenylazo)isophthalate
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  50. Procedure for generation of catalyst-free PE-TG profiles and its consequence on calculated activation energies
  51. DSC study of glycerol-extracted muscle fibers in intermediate states of ATP hydrolysis
  52. Heat capacity of indium nitride
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  54. A kinetic analysis of thermal decomposition of polyaniline and its composites with rare earth oxides
  55. A low-temperature heat capacity study of natural lithium micas
  56. Synthesis, structural and thermal characterization of metaphosphatecobalt(II) salt
  57. Temperature dependences of solid structure and properties of biodegradable poly(butylene succinate- co -terephthalate) (PBST) copolyester
  58. Sodium, zinc and magnesium chlorides as additives for soybean hulls pyrolysis
  59. Palladium(II) complexes with 5-methyl-5-(4-pyridyl)-2,4-imidazolidenedione
  60. The effect of trimethylamine N-oxide on RNase a stability
  61. Assessment of the antioxidant effect of ethanol extract of Allium sativum L., isolated and/or synergistically associated with synthetic antioxidants, applied to linseed oil
  62. The removal of template from SBA-15 samples synthesized from different silica sources
  63. Studies on the equilibrated thermodesorption of n -hexane from ZSM-5 zeolite
  64. DSC kinetic study of the incompatibility of doxepin with dextrose
  65. Expanded graphite
  66. Elaborated molecular docking and DFT/B3LYP studies for novel sulfa drug complexes, spectral and antitumor investigations
  67. Thermal and quality evaluation of vegetable oils used in ruminant feed
  68. Improved mechanical property, thermal performance, flame retardancy and fire behavior of lignin-based rigid polyurethane foam nanocomposite
  69. Evaluation of specific heat and related thermodynamic properties of Ge 1− x Sn x Se 2.5 (0 ≤  x ≤ 0.5) glasses
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  72. Comparison of rhodamine B degradation under UV irradiation by two phases of titania nano-photocatalyst
  73. Editorial 2015
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  75. Cross-linking epoxide resins with hydrolysates of chrome-tanned leather waste
  76. Thermochemical study on ternary complex of dysprosium m -nitrobenzoic acid with o -phenanthroline
  77. Standard molar enthalpies and entropies of vaporization for twolow-melting trichlorophenoxy herbicides
  78. Heats of solution in water of salts of the type R 4 NBr and R 2 R′ 2 NBr
  79. The back-titration of chemisorbed atomic oxygen on copper by carbon monoxide investigated by microcalorimetry and transient kinetics
  80. Growth and characterization of semiorganic crystal
  81. Thermal behaviour of dimethylgold(III) carboxylates
  82. Thermogravimetric study of 8-hydroxyquinoline 5-sulfonic acid–melamine–formaldehyde terpolymer resins-II
  83. Reduction of lead and zinc sulphates by hydrogen
  84. On evaluate of the integral methods for the determination of the activation energy
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  87. Flame spread over n -butanol at sub-flash temperature in normal and elevated altitude environments
  88. Multifactorial cycling performance of Cyclists and Non-Cyclists and their effect on skin temperature
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  91. Thermodynamics of mixed-ligand complex formation of copper (II) ethylenediaminetetraacetate with hexamethylenediamine in an aqueous solution
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  93. Thermal hazard investigation of cumene hydroperoxide in the first oxidation tower
  94. Crystallization kinetics of Ti 20 Zr 20 Cu 60 metallic glass by isoconversional methods using modulated differential scanning calorimetry
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  106. Hydrogen absorption kinetics of V–Al alloy
  107. Thermal stability and degradation of binuclear hexaaqua-bis(ethylenediamine)-( μ 2 -pyromellitato)dinickel(II) tetrahydrate
  108. A DSC study of precipitation hardening in a WE43 Mg alloy
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  111. Thermal stability of metastable nano-composites in planar flow cast Ti–Zr–Ni alloys
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