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Title of Journal: J Therm Anal Calorim

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Abbravation: Journal of Thermal Analysis and Calorimetry

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Springer Netherlands

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DOI

10.1016/j.ajog.2016.05.006

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ISSN

1588-2926

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TG–DTA XRD SEM EDX UV and FTIR spectroscopic

Authors: M K Sangeetha M Mariappan G Madhurambal S C Mojumdar
Publish Date: 2014/09/04
Volume: 119, Issue: 2, Pages: 907-913
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Abstract

A new semi organic nonlinear optical NLO crystal lvaline thiourea has been synthesized and good optical quality single crystals were grown by slow evaporation technique The growth conditions of the crystals are studied and the grown crystals are confirmed by powder Xray diffraction studies The grown crystal was characterized using powdered XRD FTIR UV–Vis–NIR EDX and TG–DTA The crystalline nature and its various planes of reflections were observed by the powder XRD The presence of various functional groups was confirmed by FTIR spectra The UV–Vis–NIR spectra indicate that the crystal has very good absorption in the entire visible and near IR region spectrum suggesting the suitability of the material for NLO applications The decomposition temperatures and mass loss have been estimated from the thermogravimetric analysis

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