Paper Search Console

Home Search Page About Contact

Journal Title

Title of Journal: Food Anal Methods

Search In Journal Title:

Abbravation: Food Analytical Methods

Search In Journal Abbravation:

Publisher

Springer US

Search In Publisher:

DOI

10.1016/0032-3861(74)90031-7

Search In DOI:

ISSN

1936-976X

Search In ISSN:
Search In Title Of Papers:

Determination of Soluble Calcium and Phosphorus in

Authors: Paul W Johns Steven R Dimler Julie J Watson Maryann Tigner Paul F Caskey
Publish Date: 2015/11/17
Volume: 9, Issue: 6, Pages: 1754-1762
PDF Link

Abstract

A method for the determination of soluble calcium and soluble phosphorus in commercial milled hydroxyapatite is described The Ca and P residing in the supernatant after highspeed centrifugation of a 100  w/w suspension in pH 68 HEPES buffer are quantified by cresolphthalein and phosphomolybdenum complex colorimetry respectively Method performance has been defined by assessments of linearity r 2 averages for Ca and P respectively were 0998 ± 0001 n = 15 and 1000 ± 0000 n = 15 intermediate precision soluble Ca rsd = 12  at 0500 mg/g to 05  at 804 mg/g soluble P rsd = 18  at 00526 mg/g to 05  at 35 mg/g soluble Ca/P molar ratio rsd = 18  at 63 to 05  at 188 n = 3 days and accuracy spike recovery average = 997 ± 36  for soluble Ca and 978 ± 06  for soluble P n = 4 A hydroxyapatite milled to successively smaller particle sizes exhibited increases in soluble Ca P and Ca/P as the particle size median decreased from 2339 to 1375 μm Application of the method to seven commercial lots of milled hydroxyapatite found soluble Ca from 0118 to 198  of theoretical Ca soluble P from 0386 to 180  of theoretical P and soluble Ca/P molar from 0258 to 354 The interaction of these lots with sodium caseinate in a simulated retort model was strongly correlated with their soluble Ca concentration r 2  09 The method provides a simple and inexpensive means for identifying potentially problematic lots of milled hydroxyapatite ie lots with soluble Ca and P levels sufficiently high to adversely affect the physical stability of retort sterilized milkbased liquid nutritional productsPaul W Johns declares that he has no conflict of interest Steven R Dimler declares that he has no conflict of interest Julie J Watson declares that she has no conflict of interest Maryann Tigner declares that she has no conflict of interest Paul F Caskey declares that he has no conflict of interest

Keywords:

References

.
Search In Abstract Of Papers:
Other Papers In This Journal:
  1. High-Throughput ICP-MS and Chemometrics for Exploring the Major and Trace Element Profile of the Mediterranean Sepia Ink
  2. Selenium Speciation in Rice Samples by Magnetic Ionic Liquid-Based Up-and-Down-Shaker-Assisted Dispersive Liquid-Liquid Microextraction Coupled to Graphite Furnace Atomic Absorption Spectrometry
  3. Improvement of Energy Dispersive X-Ray Fluorescence Throughput: Influence of Measuring Times and Number of Replicates on Validation Performance Characteristics
  4. Direct Determination of Saccharin and Acesulfame-K in Sweeteners and Fruit Juices Powders
  5. Electrochemical Determination of Carbendazim in Food Samples Using an Electrochemically Reduced Nitrogen-Doped Graphene Oxide-Modified Glassy Carbon Electrode
  6. Simultaneous Determination of Caffeine and Aspartame in Diet Supplements and Non-Alcoholic Beverages Using Liquid-Chromatography Coupled to Corona CAD and UV-DAD Detectors
  7. Recovery of Aromatic Aglycones from Grape Pomace Winemaking By-Products by Using Liquid-Liquid and Pressurized-Liquid Extraction
  8. Does the Plant Matrix Type Have Impact on Rutin Transformation During Its Extraction?
  9. Statistical Evaluation of Real-Time PCR Protocols Applied to Quantify Genetically Modified Maize
  10. An Enzymatic Method for Methanol Quantification in Methanol/Ethanol Mixtures with a Microtiter Plate Fluorometer
  11. Determination of Mineral Composition and Heavy Metal Content of Some Nutraceutically Valued Plant Products
  12. Evaluation and Optimization of a Superior Extraction Method for the Characterization of the Volatile Profile of Black Tea by HS-SPME/GC-MS
  13. Determination of Zearalanol and Its Analog Zearalanone in Muscle Tissues by Amplified Luminescent Proximity Homogeneous Assay (AlphaLISA)
  14. Validation of a HS-SPME-GC Method for Determining Higher Fatty Esters and Oak Lactones in White Rums
  15. Development of a Single Chain Variable Fragment Antibody and Application as Amatoxin Recognition Molecule in Surface Plasmon Resonance Sensors
  16. A Low-Cost and High Sensitive Paper-Based Microfluidic Device for Rapid Detection of Glucose in Fruit
  17. A Selective Chromatographic Method to Determine the Dynamic of Biogenic Amines During Brewing Process
  18. Validation of HPLC-UV Methods for the Quantification of Betaine in Foods by Comparison with LC-MS
  19. On-Vine Monitoring of Grape Ripening Using Near-Infrared Spectroscopy
  20. Detection Method Optimization, Dynamic Changes during Alcoholic Fermentation and Content Analysis of “Brett Character” Compounds 4-Ethylphenol (4-EP) and 4-Ethylguaiacol (4-EG) in Chinese Red Wines
  21. Rapid and Non-destructive Determination of Moisture Content of Peanut Kernels Using Hyperspectral Imaging Technique
  22. Analysis of Free Amino Acids in Russula griseocarnosa Harvested at Different Stages of Maturity Using iTRAQ ® -LC-MS/MS
  23. Development and Validation of a Cost-Effective HPLC-FLD Method for Routine Analysis of Fumonisins B 1 and B 2 in Corn and Corn Products
  24. Development and Validation of a Cost-Effective HPLC-FLD Method for Routine Analysis of Fumonisins B 1 and B 2 in Corn and Corn Products
  25. Rapid Determination of Tetracyclines Hydrochloride Using ATR FT-MIR Spectroscopy
  26. Analysis of Pesticide Residues and Their Variability in Cabbage Using QuEChERS Extraction in Combination with LC-MS/MS
  27. Provision of Ultrasensitive Quantitative Gold Immunochromatography for Rapid Monitoring of Olaquindox in Animal Feed and Water Samples
  28. The Mesoporous Porphyrinic Zirconium Metal-Organic Framework for Pipette-Tip Solid-Phase Extraction of Mercury from Fish Samples Followed by Cold Vapor Atomic Absorption Spectrometric Determination
  29. Analysis of Pesticide Residues and Their Variability in Cabbage Using QuEChERS Extraction in Combination with LC-MS/MS
  30. Optimized Formation, Extraction, and Determination of Sulforaphane in Broccoli by Liquid Chromatography with Diode Array Detection
  31. Determination of Haloxyfop-Methyl, Linuron, and Procymidone Pesticides in Carrot Using SLE-LTP Extraction and GC-MS
  32. Determination of Aflatoxins M1, M2, B1, B2, G1, and G2 and Ochratoxin A in UHT and Powdered Milk by Modified QuEChERS Method and Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry
  33. Preparation of Molecularly Imprinted Polymer Monolith with an Analogue of Thiamphenicol and Application to Selective Solid-Phase Microextraction
  34. A Rapid and Sensitive Method for Semicarbazide Screening in Foodstuffs by HPLC with Fluorescence Detection
  35. Evaluation of Extraction Methods for Efficient Detection of Enteric Viruses in Pork Meat Products
  36. Optimization and Application of a HS-SPME-GC-MS Methodology for Quantification of Furanic Compounds in Espresso Coffee
  37. Liquid Chromatography for the Rapid Screening of Growth Promoters Residues in Meat
  38. Direct Determination of Molybdenum in Milk and Infant Food Samples Using Slurry Sampling and Graphite Furnace Atomic Absorption Spectrometry
  39. Improvement of the Detection Sensitivity for Staphylococcus aureus in Spices and Herbs
  40. Ionic Liquid-based Ultrasound-Assisted In Situ Solvent Formation Microextraction Combined with Electrothermal Atomic Absorption Spectrometry as a Practical Method for Preconcentration and Trace Determination of Vanadium in Water and Food Samples
Search Result: