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Title of Journal: Food Anal Methods

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Abbravation: Food Analytical Methods

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Springer US

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DOI

10.1002/cne.902440309

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1936-976X

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Validation of a HSSPMEGC Method for Determining

Authors: Jorge A Pino Elda Roncal
Publish Date: 2015/12/03
Volume: 9, Issue: 7, Pages: 1958-1962
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Abstract

Higher fatty esters and oak lactones are the main components of white rum aroma and furthermore they have an important sensorial impact in these distilled alcoholic beverages A method for analyzing these volatile compounds was validated It involves a separation and concentration step using headspace solidphase microextraction HSSPME and determination by capillary gas chromatography using flame ionization detection The method showed a good withinday RSD  3  and betweenday precision RSD  5  The calibration curves were linear at the tested ranges R  099 and the limits of detection and quantification were 0001–0018 and 0003–0054 mg L−1 12  v/v alcohol respectively Good recoveries were obtained 986–1003  The method is suitable for the quality control of higher fatty esters and oak lactones in white rums

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Other Papers In This Journal:
  1. High-Throughput ICP-MS and Chemometrics for Exploring the Major and Trace Element Profile of the Mediterranean Sepia Ink
  2. Selenium Speciation in Rice Samples by Magnetic Ionic Liquid-Based Up-and-Down-Shaker-Assisted Dispersive Liquid-Liquid Microextraction Coupled to Graphite Furnace Atomic Absorption Spectrometry
  3. Improvement of Energy Dispersive X-Ray Fluorescence Throughput: Influence of Measuring Times and Number of Replicates on Validation Performance Characteristics
  4. Direct Determination of Saccharin and Acesulfame-K in Sweeteners and Fruit Juices Powders
  5. Electrochemical Determination of Carbendazim in Food Samples Using an Electrochemically Reduced Nitrogen-Doped Graphene Oxide-Modified Glassy Carbon Electrode
  6. Simultaneous Determination of Caffeine and Aspartame in Diet Supplements and Non-Alcoholic Beverages Using Liquid-Chromatography Coupled to Corona CAD and UV-DAD Detectors
  7. Recovery of Aromatic Aglycones from Grape Pomace Winemaking By-Products by Using Liquid-Liquid and Pressurized-Liquid Extraction
  8. Does the Plant Matrix Type Have Impact on Rutin Transformation During Its Extraction?
  9. Statistical Evaluation of Real-Time PCR Protocols Applied to Quantify Genetically Modified Maize
  10. An Enzymatic Method for Methanol Quantification in Methanol/Ethanol Mixtures with a Microtiter Plate Fluorometer
  11. Determination of Mineral Composition and Heavy Metal Content of Some Nutraceutically Valued Plant Products
  12. Evaluation and Optimization of a Superior Extraction Method for the Characterization of the Volatile Profile of Black Tea by HS-SPME/GC-MS
  13. Determination of Zearalanol and Its Analog Zearalanone in Muscle Tissues by Amplified Luminescent Proximity Homogeneous Assay (AlphaLISA)
  14. Development of a Single Chain Variable Fragment Antibody and Application as Amatoxin Recognition Molecule in Surface Plasmon Resonance Sensors
  15. A Low-Cost and High Sensitive Paper-Based Microfluidic Device for Rapid Detection of Glucose in Fruit
  16. A Selective Chromatographic Method to Determine the Dynamic of Biogenic Amines During Brewing Process
  17. Validation of HPLC-UV Methods for the Quantification of Betaine in Foods by Comparison with LC-MS
  18. On-Vine Monitoring of Grape Ripening Using Near-Infrared Spectroscopy
  19. Detection Method Optimization, Dynamic Changes during Alcoholic Fermentation and Content Analysis of “Brett Character” Compounds 4-Ethylphenol (4-EP) and 4-Ethylguaiacol (4-EG) in Chinese Red Wines
  20. Rapid and Non-destructive Determination of Moisture Content of Peanut Kernels Using Hyperspectral Imaging Technique
  21. Analysis of Free Amino Acids in Russula griseocarnosa Harvested at Different Stages of Maturity Using iTRAQ ® -LC-MS/MS
  22. Development and Validation of a Cost-Effective HPLC-FLD Method for Routine Analysis of Fumonisins B 1 and B 2 in Corn and Corn Products
  23. Development and Validation of a Cost-Effective HPLC-FLD Method for Routine Analysis of Fumonisins B 1 and B 2 in Corn and Corn Products
  24. Determination of Soluble Calcium and Phosphorus in Commercial Milled Hydroxyapatite
  25. Rapid Determination of Tetracyclines Hydrochloride Using ATR FT-MIR Spectroscopy
  26. Analysis of Pesticide Residues and Their Variability in Cabbage Using QuEChERS Extraction in Combination with LC-MS/MS
  27. Provision of Ultrasensitive Quantitative Gold Immunochromatography for Rapid Monitoring of Olaquindox in Animal Feed and Water Samples
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  29. Analysis of Pesticide Residues and Their Variability in Cabbage Using QuEChERS Extraction in Combination with LC-MS/MS
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  33. Preparation of Molecularly Imprinted Polymer Monolith with an Analogue of Thiamphenicol and Application to Selective Solid-Phase Microextraction
  34. A Rapid and Sensitive Method for Semicarbazide Screening in Foodstuffs by HPLC with Fluorescence Detection
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  36. Optimization and Application of a HS-SPME-GC-MS Methodology for Quantification of Furanic Compounds in Espresso Coffee
  37. Liquid Chromatography for the Rapid Screening of Growth Promoters Residues in Meat
  38. Direct Determination of Molybdenum in Milk and Infant Food Samples Using Slurry Sampling and Graphite Furnace Atomic Absorption Spectrometry
  39. Improvement of the Detection Sensitivity for Staphylococcus aureus in Spices and Herbs
  40. Ionic Liquid-based Ultrasound-Assisted In Situ Solvent Formation Microextraction Combined with Electrothermal Atomic Absorption Spectrometry as a Practical Method for Preconcentration and Trace Determination of Vanadium in Water and Food Samples
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