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Title of Journal: J Mater Sci Mater Electron

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Abbravation: Journal of Materials Science: Materials in Electronics

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Springer US

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DOI

10.1016/0002-9378(75)90059-9

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1573-482X

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Microstructural and electrical properties of PbTIO

Authors: P B A Fechine M J S da Rocha M R P Santos F M M Pereira A S de Menezes J M A Almeida J C Góes A P Ayala A S B Sombra
Publish Date: 2007/10/25
Volume: 19, Issue: 10, Pages: 973-980
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Abstract

In this article we will study the structural and electrical properties of PbTiO3 PTO screenprinted thick films These properties can change with synthetic routes employed for synthesis of PTO The ceramic powder has been synthesized by mechanical alloying and solid state route This material crystallizes in the tetragonal system with space group P4mm and unit cell dimensions a = b = 3904 c = 4152 Å and Z = 1 From our results it was observed that PTO obtained by mechanical alloying provides smaller crystallite size The Rietveld refinement showed that the samples synthesized by mechanical alloying and solid state route crystallize in the tetragonal system but with different cell parameters The Raman shifts of these films agree with modes from literature However some displacements happen because the morphology and structural characteristics of the thick films are different compared to single crystal and thin film The photomicrographs of the PTO thick films showed that the choice of synthetic routes obtained samples with different microstructures

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