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Title of Journal: Journal of Elec Materi

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Abbravation: Journal of Electronic Materials

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Springer US

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DOI

10.1007/s00436-013-3437-9

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1543-186X

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Preparation Characterization and Ionic Transport

Authors: Sam Solomon Aneesh George Jijimon Kumpakkattu Thomas Annamma John
Publish Date: 2014/10/31
Volume: 44, Issue: 1, Pages: 28-37
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Abstract

Nanoparticles of lanthanide Lnbased zirconates have been prepared through the autoignited combustion technique The structure of the system was analyzed by powder xray diffraction and vibrational spectroscopic tools The compounds with Ln = Ce Pr Nd Sm and Gd have pyrochlore cubic structure whereas those with Ln = Dy Er and Yb possess aniondeficient disordered cubic fluorite structure The optical properties of the powder were analyzed using ultraviolet–visible spectroscopy Pellets of the compounds were sintered in the range from 1325°C to 1530°C for 2 h The surface morphology of sintered Nd2Zr2O7 was analyzed by scanning electron microscopy Impedance spectroscopic studies of the samples were carried out at different temperatures The conductivity increased to the order of 10−2 S/m at 750°C and the highest conductivity of 1321 × 10−2 S/m was obtained for Er2Zr2O7 All samples of this system are suitable candidates for fabrication of electrolytes for use in solid oxide fuel cells particularly at moderate temperatures

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